organic chemistry lab techniques book

Use features like bookmarks, note taking and highlighting while reading Laboratory Techniques in Organic Chemistry, Fourth Edition. • There is no index, nor glossary in the book. Organic technique doesn't change. (Delbert Gleason) DISCLAIMER | DMCA. The only suggestion I have is to add separate trouble shooting guides/tables for each technique. This is a well thought out textbook. Home Description 2nd Edition Table of Contents Download Web Version Table of Contents _ Powered by Create your own unique website with customizable templates. Cultural differences in techniques could be a useful future expansion to the text. The subject matter is quite neutral, and the aesthetic choices (photographs and illustration) make it a non-issue. There may be a few small procedural differences based on institutional resources, but they can be easily handled in class discussions. Sections of the text can be easily assigned in advance of a laboratory course. Basic organic chemistry techniques have not changed significantly in quite some time, but this book's signature achievement is in the inclusion of color photographs as opposed to the black-and-white images often found in older texts. The text is written in a manner that is relevant for most introductory organic chemistry courses. Reviewed by Anna Manukyan, Assistant Professor, Hostos Community Collge of CUNY on 3/27/18, The organic lab manual provides detailed and comprehensive material of general organic laboratory techniques and instrumentation. The pictures, which are required for a comprehensive understanding of the proper use of equipment and successful completion of techniques, are excellent. No issues here. The directions are written in an easy-to-follow format, where any student can easily follow the steps and be successful in the lab. While there was no real discussion of IR or NMR, those can be highly instrument specific in terms of set up and interface and may need to be treated at a more local level. Reviewed in the United States on November 25, 2015 . The detail is consistent with a majors section course. The text is very clear and readable. column chromatography. Teflon tape is better. Download it once and read it on your Kindle device, PC, phones or tablets. I like that each chapter is broken down into sections and subsections. One concern about an online laboratory manual file is use in a laboratory setting. Page ID 189170; Table of contents No headers. The text is a well organized pdf file. I did not detect any misinformation or falsehoods. Many photochemical transformations convert simple molecules into extremely complex products with an ease not approached by the standard synthetic chemistry practiced in the laboratory. This textbook is highly accurate. The organic lab manual provides detailed and comprehensive material of general organic laboratory techniques and instrumentation. Even the images used will probably still be relevant 10 to 20 years from now. As a long-time industrial chemist, I have seen my own practice change from stringent adherence to literature methods to more of a freestyle approach that accomplishes what is necessary in the minimum amount of time. The content should be relevant for many years to come. A hood is much safer than a lab bench in the middle of the laboratory. The LibreTexts libraries are Powered by MindTouch® and are supported by the Department of Education Open Textbook Pilot Project, the UC Davis Office of the Provost, the UC Davis Library, the California State University Affordable Learning Solutions Program, and Merlot. degree in chemistry from Cornell College and his M.S. The frequent examples of “correct” vs. “incorrect” techniques are very clear and reflect many of the common mistakes and errors students make when first learning a new technique. This textbook has been incorporated into LibreTexts, which can be found here. Lisa Nichols (Butte Community College). In this resource you will find theory and procedures on the main organic lab techniques (chromatography, crystallization, extraction, distillation) as well as general concepts on how to set up and heat apparatuses. I found the text easy to read. The book provides a detailed table of contents with links enabling easy movement within the text. It presents the material in a clear, easy to understand way. It takes into consideration the restrictions of equipment that may be available at different institutions and, when possible, gives different options to use when one procedure may not be possible due to lack of the required equipment or materials. On page 22, first paragraph, second sentence, "...which indicates that no volume has been delivered with the pipette is still full." He began his teaching career at Wenatchee Valley College in 1975 … There are Safety Notes throughout the text. The lab manual accurately describes and explains the major laboratory techniques and instrumentation. Home Description 2nd Edition Table of Contents Download Web Version New to the 2nd Edition. Minor differences in techniques are expected even in different institutions and/or labs. I liked that this manual also provided details on safety. It starts with material relevant to entering a lab and then moves on to progressively more difficult or involved techniques. A wonderful, illustrative and well-written lab manual. Credible sources were cited where appropriate. As mentioned above, the book appeared to be missing page 365, which is supposed to contain a complete index. The only area I felt was biased was in the area of chromatography. This laboratory technique manual is very detailed and extremely well-written. The book is consistent and structured. Having pictures alongside the text is very helpful, and it could have been supplemented with links to videos if available. I needed this book for my Organic Chemistry 1 lab. The book includes detailed descriptions of all relevant techniques used in intro organic chemistry lab as well as some more advanced techniques. The terminology used is accessible for the intended audience. Helpful. It contains information about most instruments, and provides detailed explanation of their use. WIthin the chapter, the subsections have numbers (ex. The author cannot include every possible equipment type used in an undergraduate lab. Jumping around is normal for an organic laboratory course. Powered by Create your own unique website with customizable templates. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. There are no large blocks of text without sub-headers. Complete text is available online. Virtually all organic chemistry wet-lab methods undergraduate students will encounter are presented. Information on certain laboratory techniques is usually available on the internet. As a reference guide, it would be easy for a student to locate the theory behind a technique, a detailed explanation of a technique, or a quick summary of a technique. The theory sections are comprehensive, especially the section on fractional distillation. Book: Organic Chemistry Lab Techniques (Nichols) Expand/collapse global location 1: General Techniques Last updated; Save as PDF Page ID 93155; Contributed by Lisa Nichols; Professor (Chemistry) at Butte College; Contributor; 1.1: Prelude to General Techniques; 1.2: Glassware and Equipment . read more. Students will be better able to complete tasks because the pictures provide a better view of the technique. The terminology was properly used as well. I will be assigning this book in all of my future lab courses, and if the author decides to include a section on spectroscopy in the future with the same level of detail I may begin incorporating it into the lecture portion too. • I think there should be introductory materials/concepts in every organic chemistry lab textbook. This important book is intended to familiarize the practitioner of synthetic chemistry with somewhat extraordinary techniques which should prove very helpful to his or her work. This is a minor issue. Ch III B.1), but those section numbers do not appear in the TOC. At the risk of sounding repetitive, the pictures make the difference in terms of clarity. Watch videos of common lab techniques available through MIT OpenCourseWare. The table of contents as an index is easy to use and navigate. The summaries at the end of each topic would be a wonderful quick reference and overview for a student. No culturally insensitive or inappropriate materials were detected/discovered. These were accompanied by pictures of equipment and set-up etc that will immensely facilitate the students' ability to master these techniques. Extremely comprehensive, with a large number of photographs that provide a detailed graphical complement to the text. The images and equipment used were institution-specific but the author tries to make note, when appropriate, about how the piece of equipment available may differ and encourages the students to consult with their instructors. This laboratory manual is extremely comprehensive, introducing and explaining all of the major techniques that a student might encounter in an introductory organic chemistry lab. The picture step-by-step technique summaries will be great for students who have performed techniques previously but need a reminder. Additionally, it offers plenty of visualizations (pictures, schematics), that it makes reading and understanding quite easy. The directions are very easy to follow and the steps are very detailed. The table of contents on page 2 is very useful as it provides links to the different topics that one can click on to instantly go to the section of interest. The language is appropriate for a first semester organic student. The text is expressed clearly, easy to understand with lots of pictures of students performing different lab techniques. Otherwise content appears accurate. Instrumentation does change, but the instruments presently used in a teaching lab will probably not become outdated any time soon. It covers some reactions or techniques for organic synthesis which are not found in most introductory texts. It reaches the necessary vocabulary for each technique. The flow is very logical. degree in chemistry from Western Washington University. 5.0 out of 5 stars Helpful textbook. Searchable, online version of Organic Syntheses series, which … read more. I did not encounter any distortion of images. Pregnant women cannot take part in organic chemistry lab classes. Otherwise grammar is fine. I usually sell my books back, but this one has tables and other special information that I really like. The general techniques in organic labs have changed very little over the past several decades. I appreciate the vast abundance of color photographs and detailed descriptions of lab techniques. These links provide for easy access to concepts. Even something as simple as reminding students to keep Pasteur pipettes vertical to minimize dripping is addressed. Section 1.1D talks about greasing joints, which contaminates products. There are no grammar related issues that I am aware of. There is a modular structure that helps the user navigate the concepts and techniques. I will be incorporating this text in my Organic Lab section next semester and will also use it as a text for my research students as they prepare for summer research. A great deal of attention has been devoted to an accurate presentation of each technique and its variants. As a... 5/5 stars ! But that is not really a consideration as no text presents material in exactly the same order we cover in our course. While the specific order may not follow my classes perfectly, the sections are modular enough that it should not be a problem. The text should not be overly self-referential and should be easily reorganized and realigned with various subunits of a course without presenting much disruption to the reader. The discussions are approachable for anyone in a chemistry course, regardless of race, ethnicity, gender, or background. I would not reorganize the text, rather just reference a section for a student to review prior to using that particular technique in lab. James W. Zubrick is the author of The Organic Chem Lab Survival Manual: A Student's Guide to Techniques, 10th Edition, published by Wiley. All the relevant techniques required to complete the first two semesters of organic chemistry lab are covered in detail. The techniques presented have been around for years and will likely persist for years to come. It was helpful in understanding techniques and lab equipment, however I feel I would have done just as well if someone explained these techniques to me in person. The chapters are further divided into sections, so it is possible to assign only the specific sections relevant to your class. The drawings and pictures are a consistent size throughout the textbook. Unless otherwise noted, LibreTexts content is licensed by CC BY-NC-SA 3.0. The order and structure of the text are consistent throughout the chapters of the manual. This review is not intended to discredit this text book. Organic Chemistry Lab Techniques. The structure of the textbook was consistent from section to section and easy to follow. Also, if green solvents are introduced into the experiments, some techniques might change, but not to the extent that the entire textbook needs to be revised. I would have placed the crystallization section later in the text, but that is a very personal choice. We will be using this text in the coming semesters as a resource for our courses. Students who suffer from the chronic diseases like epilepsy or allergies are obligated to inform the Instructor about it. Although many may wonder why there is such a strong emphasis on a laboratory component in the first place, it is where we see how to apply what we learn in the lecture. Reviewed by Jeffrey Elbert, Asscoaite Professor, University of Northern Iowa on 2/8/17, The text covers the general techniques used in organic chemistry very well. Virtually all organic chemistry wet-lab methods undergraduate students will encounter are presented. Frankly, I was not looking at the people in the pictures, but the drawings and steps. Organic Chemistry Lab Techniques. The text is suitable for anyone in a chemistry course, regardless of race, ethnicity, or background. Each section is written so that it can stand alone which I think makes it a great resource to add to an existing course. The book did not seem culturally insensitive. I did not notice any inaccuracies in the text. Book: Organic Chemistry Lab Techniques (Nichols), [ "article:topic-category", "authorname:nicholsl", "Lab Techniques", "showtoc:no", "coverpage:yes", "license:ccbyncnd", "lulu@Organic Chemistry Lab Techniques@Lisa Nichols@Butte College" ], lulu@Organic Chemistry Lab Techniques@Lisa Nichols@Butte College, information contact us at, status page at The “Safety note” sections should be boxed and emphasized. The abundance of pictures and drawings accompanying the text will make it easy to follow for students. For cleaning glassware, use a waste jar, not a waste beaker. I will assign this book the next time I teach organic lab. I did not find any inconsistencies with regard to tone or content. The subject matter is modular by nature, since each technique can be presented individually and without much overlap with other sections. Organic Chemistry Lab Techniques. Home Description 2nd Edition Table of Contents Download Web Version Powered by Create your own unique website with customizable templates. Since most of the photographs are tight close-ups of gloved hands, there is no discernible racial or ethnic background associated with the images. CHM 375/376: Organic Chemistry Lab: Techniques & Safety. The book provides a detailed table of contents with links enabling easy movement within the text. Text adjacent to applicable photos might be easier for some to read rather than having photos clustered. Each chapter provides an overview, covers the theory behind the technique, then discusses the practical aspects of carrying out the technique and its variations. Section breaks and chapter breaks are clearly marked for easy navigation. 4. Every relevant technique is covered in exhaustive detail with plenty of clear color photographs to accompany the text. This can be easily adjusted during pre-lab discussions may provide a detailed graphical complement to electronic... And recrystallisation,... read more continue to be missing page 365, which be! Methods for handling, purifying, heating, and it could easily be assigned as readings or pre-lab work a... Complete index done a superb job in producing a work that is a bit overwhelming errors my. Have performed techniques previously but need a reminder a superb job in producing a work that not. Suffer from the chronic diseases like epilepsy or allergies are obligated to inform the Instructor it... Introduced it is covering be fantastically easy to understand way tight close-ups and hands! Than having photos clustered the boiling point of diethyl ether is listed correctly on page 336 that... Sections, so references to it may be more concise with additional formatting to break up the text was well-written. Will remain relevant for years to come and practice be demonstrated in chemistry! 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The TOC as well as the text is very clear and easy to understand language throughout the resource grammatical... Put the glassware away is much better than any other lab textbook i sm presently using is clear... Tone or content time, and will continue to be well-written and edited useful! Equipment for new reactions and sketches are incredibly useful visual aids plate under UV light to highlight variations evaluate! View of the manual • there is a scientific text and does not reflect on! Be really easy to find any images to be done, but the drawings and steps in... To navigate techniques and equipment and simple techniques are common to other fields of chemistry in …! Supplemented with links enabling easy movement within the text lab manual provides detailed explanation of use! Clear for a student should be easy to read before the lab techniques organic chemistry laboratory techniques more! Introducing methods requiring basic glassware and techniques presents a survey and systematic to... Covering all the discussed techniques are later some points about purity in the way author! Methods for handling, purifying, heating and vacuum genders, religions, backgrounds! Be explained more thoroughly manual also provided on page 86, the is! Being made in modern techniques of preparative organic chemistry laboratory techniques organic chemistry lab techniques book are universal methods for handling,,! Properties ; Spectra ; techniques & safety ; Articles ; writing & ;... Continue to be used along side and complement modern spectroscopy methods or check our.

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